Arsenic contamination in water demands effective, low-cost removal methods. This study introduces nanomagnetite-coated biochar derived from pecan nutshells for efficient arsenic adsorption. Utilizing a solvothermal method, uniform magnetite crystals were grown on biochar in a controlled process at 200 ◦C. The resulting bioadsorbent, characterized by XRD, SEM, and FTIR, exhibited a narrow size distribution and consistently high arsenic removal rates (97.30–98.76%). Biochar with varied particle sizes, synthesized at a short reaction time (6 h), showed the highest removal efficiency of arsenic (98.76%) and adsorption capacity (7.974 mg/g). This approach offers a sustainable for arsenic remediation, and ease of magnetic separation.
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